3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

Base Information

Chemical Name:3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt
CAS No.:1123546-32-6
Molecular Formula:C₂HF₃O₂*C₁₄H₁₈F₃N₃O₃
Molecular Weight:447.334
Hs Code.:

Synonyms:3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

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Chemical Property of 3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

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Technology Process of 3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

There total 1 articles about 3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1123546-42-8
2-[3-(N'-tert-butoxycarbonylhydrazino)-4,4,4-trifluorobutyrylamino]-3-phenyl-propionic acid methyl ester

: 76-05-1
trifluoroacetic acid

: 1123546-32-6
3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2008.11.012

Reference yield: 77.0%

: 1123546-32-6
3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

: 1758-25-4
(2,5-dimethoxyphenyl)acetic acid

: 2-(3-{N'-[2-(2,5-dimethoxy-phenyl)-acetyl]-hydrazino}-4,4,4-trifluoro-butyrylamino)-3-phenyl-propionic acid methyl ester

Guidance literature:: 3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt; With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

(2,5-dimethoxyphenyl)acetic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.ejmech.2013.09.059

Reference yield: 63.0%

: 1123546-32-6
3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt

: 7536-55-2
N-tert-butyloxycarbonylasparagine

: 2-{3-[N'-(2-tert-butoxycarbonylamino-3-carbamoyl-propionyl)-hydrazino]-4,4,4-trifluoro-butyrylamino}-3-phenyl-propionic acid methyl ester

Guidance literature:: 3-phenyl-2-(4,4,4-trifluoro-3-hydrazinobutyrylamino)propionic acid methyl ester trifluoroacetic acid salt; With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

N-tert-butyloxycarbonylasparagine; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.ejmech.2013.09.059