Technology Process of C22H24ClFN4O4
There total 9 articles about C22H24ClFN4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 0 °C
2: pyridine / dichloromethane / 2 h
3: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
With
pyridine; triethylamine; HATU;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 94 h / 20 - 60 °C / Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 4.5 h / 0 - 20 °C
3: methanol / 3 h / 40 °C
4: borane-THF / tetrahydrofuran / 28 h / 90 °C
5: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
With
borane-THF; sodium tris(acetoxy)borohydride; triethylamine; HATU; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;