N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide

Base Information

Chemical Name:N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide
CAS No.:1293973-91-7
Molecular Formula:C₂₄H₂₁N₅O₂
Molecular Weight:411.463
Hs Code.:

Synonyms:N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide

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Chemical Property of N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide

Chemical Property:

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Technology Process of N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide

There total 2 articles about N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1293973-89-3
4-(4-phenyl-[1,2,3]-triazol-1-yl)-1,8-naphthalic anhydride

: 108-00-9
N,N-dimethylethylenediamine

: 1293973-91-7
N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1016/j.ejmech.2011.01.050

Reference yield:

: 81-86-7
4-bromo-1,8-naphthalenedicarboxylic anhydride

: 1293973-91-7
N-(2-(dimethylamino)ethyl)-4-(4-phenyl-[1,2,3]-triazol-1-yl)-naphthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / water; N,N-dimethyl-formamide / 5 h / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol

3: ethanol / 3 h / Reflux

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2: Huisgen cycloaddition;
DOI:10.1016/j.ejmech.2011.01.050