1--1-phenylamino-aethan

Base Information

Chemical Name:1--1-phenylamino-aethan
CAS No.:94256-56-1
Molecular Formula:C₁₉H₁₇NO
Molecular Weight:275.35
Hs Code.:

Synonyms:1--1-phenylamino-aethan

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Chemical Property of 1--1-phenylamino-aethan

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Technology Process of 1--1-phenylamino-aethan

There total 5 articles about 1--1-phenylamino-aethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62244-84-2
β-naphthacylaniline

: 74-88-4
methyl iodide

: 94256-56-1
1--1-phenylamino-aethan

Guidance literature:: β-naphthacylaniline; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 3h;
DOI:10.1016/j.tet.2016.12.069

Reference yield:

: 76469-34-6
2-bromo-1-(2-naphthyl)-1-propanone

: 94256-56-1
1--1-phenylamino-aethan

Guidance literature:: Multi-step reaction with 3 steps

1: silver tetrafluoroborate / 1,2-dichloro-ethane / 24 h / 85 °C / Inert atmosphere; Schlenk technique

2: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

3: 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate / Inert atmosphere

With silver tetrafluoroborate; 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane; mineral oil;
DOI:10.1021/jacs.0c07210

Reference yield:

: (1-(naphthalen-2-yl)-1-oxopropan-2-yl)diphenylsulfonium tetrafluoroborate

: 94256-56-1
1--1-phenylamino-aethan

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

2: 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate / Inert atmosphere

With 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1021/jacs.0c07210