(3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

Chemical Name:(3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
CAS No.:352285-09-7
Molecular Formula:C₁₅H₃₀N₂O₂
Molecular Weight:270.415
Hs Code.:

Synonyms:(3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Chemical Property of (3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Technology Process of (3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 2 articles about (3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16832-20-5,32815-12-6,55284-67-8
(1R,2S,5R)-menthol bromoacetate

: 109-76-2,54018-94-9
Trimethylenediamine

: 352285-09-7
(3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ja010249w

Reference yield:

: 2216-51-5
(-)-menthol

: 352285-09-7
(3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: EDC; DMAP / CH₂Cl₂ / 0 - 20 °C

2: DIPEA / tetrahydrofuran / 0 - 20 °C

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja010249w

Reference yield:

: 210769-64-5
pentamethylene bis[4-(10,15,20-triphenylporphin-5-yl)benzoate]dizinc(II)

: 352285-09-7
(3-Amino-propylamino)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: Zn(C₆H₅)3C₂₀H₈N₄C₆H₄COO(CH₂)5OCOC₆H₄C₂₀H₈N₄(C₆H₅)3Zn(NH₂(CH₂)3NHCH₂COOCHCH(CH(CH₃)2)CH₂CH₂CH(CH₃)CH₂)

Guidance literature:: In dichloromethane; soln. of ligand (ca. 30 equiv.) in CH2Cl2 added to soln. of Zn complex in CH2Cl2; not isolated; detd. by UV-vis and circular dichroism spectra;
DOI:10.1021/ja010249w