diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate

Base Information

• Chemical Name: diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate
• CAS No.: 695171-95-0
• Molecular Formula: C₃₃H₃₅N₂O₇P
• Molecular Weight: 602.624

Synonyms:diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate

Chemical Property of diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate

Chemical Property:

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Technology Process of diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate

There total 10 articles about diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

triphenyl phosphite (101-02-0) + O-benzyl carbamate (621-84-1) + 4-(tert-butyloxycarbonylamino)phenylacetaldehyde (695171-91-6) → diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate (695171-95-0)

Guidance literature:

With yttrium(III) trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 8h; chemoselective reaction; Inert atmosphere;

DOI:10.1039/d1ra07718j

Reference yield: 30.0%

triphenyl phosphite (101-02-0) + O-benzyl carbamate (621-84-1) + 4-((tert-butoxycarbonyl)amino)benzaldehyde (144072-30-0) → diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate (695171-95-0)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/jm0499209

Reference yield:

triphenyl phosphite (101-02-0) + C13H17NO2 + O-benzyl carbamate (621-84-1) → diphenyl 1-benzyloxycarbonylamino-2-(4-(tert-butyloxycarbonylamino)phenyl)ethanephosphonate (695171-95-0)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/jm700962j

upstream raw materials:

triphenyl phosphite

O-benzyl carbamate

4-((tert-butoxycarbonyl)amino)benzaldehyde

4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Downstream raw materials:

diphenyl 1-(benzyloxycarbonylamino)-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

diphenyl 1-(((N-benzyloxycarbonyl-O-tert-butyl-D-seryl)-L-alanyl)amino)-2-(4-(N,N'-bis(tert-butyloxycarbonyl)guanyl)phenyl)ethanephosphonate

diphenyl 1-((N-benzyloxycarbonyl-L-alanyl)amino)-2-(4-(N,N'-bis(tert-butyloxycarbonyl)guanyl)phenyl)ethanephosphonate

diphenyl 1-benzyloxycarbonylamino-2-(4-(N,N'-bis(tert-butyloxycarbonyl)guanyl)phenyl)ethanephosphonate

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