4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Base Information

Chemical Name:4-(tert-butyloxycarbonylamino)phenylacetaldehyde
CAS No.:695171-91-6
Molecular Formula:C13H17NO3
Molecular Weight:235.283
Hs Code.:
Mol file:695171-91-6.mol

Synonyms:tert-butyl 4-(2-oxoethyl)phenylcarbamate;tert-butyl N-[4-(2-oxoethyl)phenyl]carbamate;[4-(2-Oxo-ethyl)-phenyl]-carbamic acid tert-butyl ester;tert-butyl (4-(2-oxoethyl)phenyl)carbamate;

Suppliers and Price of 4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(4-(2-oxoethyl)phenyl)carbamate 95+%
1g
$ 412.00

Alichem
Tert-butyl(4-(2-oxoethyl)phenyl)carbamate
1g
$ 464.28

Alichem
Tert-butyl(4-(2-oxoethyl)phenyl)carbamate
250mg
$ 190.75

Total 6 raw suppliers

Chemical Property of 4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Chemical Property:

PSA：55.40000
LogP:2.84800

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(4-(2-oxoethyl)phenyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(tert-butyloxycarbonylamino)phenylacetaldehyde

There total 9 articles about 4-(tert-butyloxycarbonylamino)phenylacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 897648-31-6
ethyl 2-(4-((tert-butoxycarbonyl)amino)phenyl)acetate

: 695171-91-6
4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; Inert atmosphere;
DOI:10.1021/jm401318w

Reference yield: 94.0%

: 104060-23-3
tert-butyl N-[4-(2-hydroxyethyl)phenyl]carbamate

: 695171-91-6
4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Guidance literature:: With oxalyl dichloride; In dichloromethane; dimethyl sulfoxide; at -60 ℃; for 1.5h;
DOI:10.1021/jm4005972

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 695171-91-6
4-(tert-butyloxycarbonylamino)phenylacetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dioxane / 20 °C

2: Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With Dess-Martin periodane; triethylamine; In 1,4-dioxane; dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1021/jm060622g