(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

Base Information

Chemical Name:(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene
CAS No.:626255-53-6
Molecular Formula:C₄₃H₅₉NO₆
Molecular Weight:685.945
Hs Code.:

Synonyms:(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

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Chemical Property of (E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

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Technology Process of (E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

There total 1 articles about (E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2609-49-6
diethyl p-nitrobenzylphosphonate

: (E)-4-{4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

: 626255-53-6
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

Guidance literature:: diethyl p-nitrobenzylphosphonate; With potassium tert-butylate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

(E)-4-{4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/ja0211050

Reference yield: 70.0%

: 626255-53-6
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

: 626255-54-7
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}aniline

Guidance literature:: With tin(ll) chloride; In ethanol; ethyl acetate; at 75 ℃; for 5h;
DOI:10.1021/ja0211050

Reference yield:

: 626255-53-6
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}nitrobenzene

: (E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / aq. SnCl₂ / ethanol; ethyl acetate / 5 h / 75 °C

2: 100 percent / CHCl₃ / 0.5 h / 20 °C

3: 100 percent / LiOH*H₂O / tetrahydrofuran / 15 h / 20 °C

With lithium hydroxide; tin(ll) chloride; In tetrahydrofuran; ethanol; chloroform; ethyl acetate;
DOI:10.1021/ja0211050