(E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

Base Information

Chemical Name:(E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester
CAS No.:626255-55-8
Molecular Formula:C₄₈H₆₈N₂O₇
Molecular Weight:785.077
Hs Code.:

Synonyms:(E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

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Chemical Property of (E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

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Technology Process of (E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

There total 4 articles about (E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 626255-54-7
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}aniline

: 2949-22-6
Glycine ethyl ester isocyanate

: 626255-55-8
(E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

Guidance literature:: In chloroform; at 20 ℃; for 0.5h;
DOI:10.1021/ja0211050

Reference yield:

: 2609-49-6
diethyl p-nitrobenzylphosphonate

: 626255-55-8
(E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuOK / dimethylformamide / 0.25 h / 20 °C

1.2: 82 percent / dimethylformamide / 4 h / 20 °C

2.1: 70 percent / aq. SnCl₂ / ethanol; ethyl acetate / 5 h / 75 °C

3.1: 100 percent / CHCl₃ / 0.5 h / 20 °C

With potassium tert-butylate; tin(ll) chloride; In ethanol; chloroform; ethyl acetate; N,N-dimethyl-formamide; 1.2: Wittig-Horner reaction;
DOI:10.1021/ja0211050

Reference yield:

: (E)-4-{4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

: 626255-55-8
(E,E)-3-[4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}phenyl]ureidoacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuOK / dimethylformamide / 0.25 h / 20 °C

1.2: 82 percent / dimethylformamide / 4 h / 20 °C

2.1: 70 percent / aq. SnCl₂ / ethanol; ethyl acetate / 5 h / 75 °C

3.1: 100 percent / CHCl₃ / 0.5 h / 20 °C

With potassium tert-butylate; tin(ll) chloride; In ethanol; chloroform; ethyl acetate; N,N-dimethyl-formamide; 1.2: Wittig-Horner reaction;
DOI:10.1021/ja0211050