methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

Base Information

Chemical Name:methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate
CAS No.:1335116-43-2
Molecular Formula:C₂₃H₂₂F₃NO₅S
Molecular Weight:481.493
Hs Code.:

Synonyms:methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

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Chemical Property of methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

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Technology Process of methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

There total 8 articles about methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1335116-73-8
methyl 3-methyl-6-[(1-methylethyl)thio]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

: 1335116-43-2
methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield: 90.0%

: 1335116-46-5
methyl 6-bromo-3-methyl-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

: propane-2-sulfinic acid sodium salt

: 74-88-4
methyl iodide

: 1335116-43-2
methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

Guidance literature:: methyl 6-bromo-3-methyl-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate; propane-2-sulfinic acid sodium salt; With copper(l) iodide; In dimethyl sulfoxide; at 50 - 120 ℃; Inert atmosphere;

methyl iodide; In dimethyl sulfoxide; at 20 ℃; for 1h;

Reference yield:

: 454-89-7
3-Trifluoromethylbenzaldehyde

: 1335116-43-2
methyl 3-methyl-6-[(1-methylethyl)sulfonyl]-7-(methyloxy)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / Reflux

1.2: 20 °C / Reflux

2.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h

2.2: 100 °C

2.3: 2 h / 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; dimethyl sulfoxide; mineral oil;