ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

Base Information

Chemical Name:ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate
CAS No.:98267-83-5
Molecular Formula:C₁₆H₂₂N₄O₄S
Molecular Weight:366.441
Hs Code.:

ethyl 4-<methyl<<(2-nitrophenyl)amino>thioxomethyl>amino>-1-piperidinecarboxylate

Synonyms:ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

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Chemical Property of ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

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Technology Process of ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

There total 1 articles about ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29976-53-2
N-ethoxycarbonyl-4-piperidone

: 98267-83-5
ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 91.4 percent / H₂ / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

2: 71 percent / ethanol / Ambient temperature

With hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00150a029

Reference yield: 95.0%

: 98267-83-5
ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

: 98245-12-6
ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

Guidance literature:: With ammonia; hydrogen; palladium on activated charcoal; In methanol; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00150a029

Reference yield:

: 98267-83-5
ethyl 4-thioxomethyl>amino>-1-piperidinecarboxylate

: 98245-06-8
[1-(4-Bromo-benzyl)-1H-benzoimidazol-2-yl]-methyl-(1-phenethyl-piperidin-4-yl)-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / H₂, ammonia / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

2: 84 percent / yellow HgO, sulfur / methanol / 2 h / Heating

3: 95 percent / 48 percent aq. hydrobromic acid / 2 h / 120 °C

4: sodium carbonate / dimethylformamide / 70 °C

5: 1.) sodium hydride / 1.) dimethyl sulfoxide, benzene, 30 min, 2.) dimethyl sulfoxide, benzene, RT, overnight

With ammonia; hydrogen bromide; hydrogen; sodium hydride; sodium carbonate; sulfur; mercury(II) oxide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00150a029