2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

Base Information

Chemical Name:2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride
CAS No.:1332848-74-4
Molecular Formula:C₁₆H₂₂ClNO₂S*ClH
Molecular Weight:364.336
Hs Code.:

Synonyms:2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

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Chemical Property of 2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

Chemical Property:

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Technology Process of 2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

There total 3 articles about 2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332848-73-3
2-cyclohexylmethyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

: 1332848-74-4
2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

Guidance literature:: With chlorosulfonic acid; In dichloromethane; at -1.8 - 35 ℃; Industry scale;

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 1332848-74-4
2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride / tert-butyl methyl ether / 2.5 h / 8.8 - 21.1 °C / Industry scale

1.2: 0.5 h / 20 °C / Industry scale

1.3: 20 °C / Industry scale

2.1: chlorosulfonic acid / dichloromethane / -1.8 - 35 °C / Industry scale

With chlorosulfonic acid; sodium tris(acetoxy)borohydride; In dichloromethane; tert-butyl methyl ether;

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 1332848-74-4
2-(cyclohexylmethyl)-1,2,3,4-tetrahydroisoquinoline-7-sulfonyl chloride hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride / tert-butyl methyl ether / 2.5 h / 8.8 - 21.1 °C / Industry scale

1.2: 0.5 h / 20 °C / Industry scale

1.3: 20 °C / Industry scale

2.1: chlorosulfonic acid / dichloromethane / -1.8 - 35 °C / Industry scale

With chlorosulfonic acid; sodium tris(acetoxy)borohydride; In dichloromethane; tert-butyl methyl ether;