O--glykolsaeureaethylester

Base Information

• Chemical Name: O--glykolsaeureaethylester
• CAS No.: 95591-62-1
• Molecular Formula: C₁₂H₁₄O₄
• Molecular Weight: 222.241
• Mol file: 95591-62-1.mol

Synonyms:O--glykolsaeureaethylester

Chemical Property of O--glykolsaeureaethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of O--glykolsaeureaethylester

There total 2 articles about O--glykolsaeureaethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

diazoacetic acid ethyl ester (623-73-4) + p-Toluic acid (99-94-5) → O--glykolsaeureaethylester (95591-62-1)

Guidance literature:

With 12Hf⁽⁴⁺⁾*16O^(2-)*4HO^(1-)*20H₂O*3C₄₈H₂₄N₄O₈^(6-)*3Ir⁽³⁺⁾*3Cl^(1-); In dichloromethane; at 20 ℃; for 0.25h;

DOI:10.1002/cctc.201800597

Reference yield:

ethyl bromoacetate (105-36-2) + p-Toluic acid (99-94-5) → O--glykolsaeureaethylester (95591-62-1)

Guidance literature:

With potassium carbonate; In acetone; Heating;

DOI:10.1039/jr9640001559

Reference yield:

O--glykolsaeureaethylester (95591-62-1) → (4-Methylbenzoyloxy)essigsaeure (91634-21-8)

Guidance literature:

With potassium hydroxide;

DOI:10.1039/jr9640001559

upstream raw materials:

ethyl bromoacetate

p-Toluic acid

diazoacetic acid ethyl ester

Downstream raw materials:

(4-Methylbenzoyloxy)essigsaeure