(3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

Base Information

Chemical Name:(3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate
CAS No.:1428540-77-5
Molecular Formula:C₁₆H₁₆F₆O₃S
Molecular Weight:402.358
Hs Code.:

Synonyms:(3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

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Technology Process of (3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

There total 3 articles about (3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 928-49-4
hex-3-yne

: 1428541-18-7
(E)-o-tolyl(4-(trifluoromethyl)styryl)-λ³-iodanyl trifluoromethanesulfonate

: 1428540-77-5
(3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

Guidance literature:: With copper(l) chloride; In 1,4-dioxane; at 50 ℃; for 12h; diastereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/ja401840j

Reference yield:

: 1073354-88-7
(E)-4,4,5,5-tetramethyl-2-(3-(trifluoromethyl)styryl)-1,3-dioxa-2-borolane

: 1428540-77-5
(3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; sodium periodate / acetone / 24 h / 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

2.3: 0.25 h / 0 °C

3.1: copper(l) chloride / 1,4-dioxane / 12 h / 50 °C / Inert atmosphere; Sealed tube

With sodium periodate; boron trifluoride diethyl etherate; ammonium acetate; copper(l) chloride; In 1,4-dioxane; dichloromethane; acetone;
DOI:10.1021/ja401840j

Reference yield:

: 698998-84-4
{(E)-2-[3-(trifluoromethyl)phenyl]vinyl}boronic acid

: 1428540-77-5
(3Z,5E)-4-ethyl-6-(4-(trifluoromethyl)phenyl)hexa-3,5-dien-3-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

1.3: 0.25 h / 0 °C

2.1: copper(l) chloride / 1,4-dioxane / 12 h / 50 °C / Inert atmosphere; Sealed tube

With boron trifluoride diethyl etherate; copper(l) chloride; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ja401840j