Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

Base Information

Chemical Name:Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester
CAS No.:221341-48-6
Molecular Formula:C₃₂H₂₉NO₂
Molecular Weight:459.588
Hs Code.:

Synonyms:Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

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Technology Process of Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

There total 2 articles about Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 577979-00-1
(3R,4S)-5-phenyl-4-[(9-phenyl-9-fluorenyl)-amino]-penten-3-ol

: 221341-48-6
Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2005.06.051

Reference yield:

: 5-phenyl-4-(9-phenyl-9H-fluoren-9-ylamino)-pent-1-en-3-one

: 221341-48-6
Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: (S)-BINAL / tetrahydrofuran / -78 °C

2: Et₃N / CH₂Cl₂ / 20 °C

With (S)-BINAL; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2005.06.051

Reference yield:

: 221341-48-6
Acetic acid (R)-1-[(S)-2-phenyl-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester

: 221341-55-5
(2S,3S,4S)-3-acetoxy-2-benzyl-4-iodo-N-(9-phenylfluoren-9-yl)pyrrolidine

: Acetic acid (2S,3S,4R)-2-benzyl-4-iodo-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

Guidance literature:: With water; iodine; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; for 3h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1039/a809083a