6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

Base Information

Chemical Name:6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose
CAS No.:131289-33-3
Molecular Formula:C₂₅H₂₅NO₁₁
Molecular Weight:515.474
Hs Code.:

Synonyms:6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

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Chemical Property of 6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

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Technology Process of 6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

There total 1 articles about 6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.3%

: 127-08-2
potassium acetate

: 131289-32-2
3-O-benzoyl-6-bromo-6-deoxy-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

: 131289-33-3
6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

Guidance literature:: With aluminum oxide; 18-crown-6 ether; In acetonitrile; for 6h; Heating;
DOI:10.1016/0008-6215(90)80140-X

Reference yield:

: 131289-33-3
6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

: 26597-73-9,2847-00-9,26623-13-2,26623-14-3,26623-16-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-ulose

Guidance literature:: Multi-step reaction with 3 steps

1: 0.1M sodium methoxide / methanol / 1 h / Ambient temperature

2: acetone

3: phosphorus pentaoxide / dimethylsulfoxide; dimethylformamide / 2.5 h / 65 °C

With phosphorus pentaoxide; sodium methylate; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(90)80140-X

Reference yield:

: 131289-33-3
6-O-acetyl-3-O-benzoyl-1,2-O-isopropylidene-5-O-p-nitrobenzoyl-β-L-idofuranose

: 582-52-5
1,2:5,6-diacetone-D-glucose

Guidance literature:: Multi-step reaction with 2 steps

1: 0.1M sodium methoxide / methanol / 1 h / Ambient temperature

2: acetone

With sodium methylate; In methanol; acetone;
DOI:10.1016/0008-6215(90)80140-X