2-acetyl-3-p-methoxyphenylthiophene oxime

Base Information

Chemical Name:2-acetyl-3-p-methoxyphenylthiophene oxime
CAS No.:1319721-11-3
Molecular Formula:C₁₃H₁₃NO₂S
Molecular Weight:247.318
Hs Code.:

Synonyms:2-acetyl-3-p-methoxyphenylthiophene oxime

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Chemical Property of 2-acetyl-3-p-methoxyphenylthiophene oxime

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Technology Process of 2-acetyl-3-p-methoxyphenylthiophene oxime

There total 3 articles about 2-acetyl-3-p-methoxyphenylthiophene oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42877-08-7
1-(3-bromothiophen-2-yl)ethanone

: 1319721-11-3
2-acetyl-3-p-methoxyphenylthiophene oxime

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 18 h / Inert atmosphere; Reflux

2: hydroxylamine hydrochloride; sodium acetate / ethanol / 18 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; In ethanol; toluene; 1: Suzuki coupling;
DOI:10.1039/c1cc12720a

Reference yield:

: 132039-45-3
2-acetyl-3-(p-methoxyphenyl)thiophene

: 1319721-11-3
2-acetyl-3-p-methoxyphenylthiophene oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 18h; Reflux;
DOI:10.1039/c1cc12720a

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1319721-11-3
2-acetyl-3-p-methoxyphenylthiophene oxime

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 18 h / Inert atmosphere; Reflux

2: hydroxylamine hydrochloride; sodium acetate / ethanol / 18 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; In ethanol; toluene; 1: Suzuki coupling;
DOI:10.1039/c1cc12720a