C₁₂H₁₇NO₄S

Base Information

Chemical Name:C₁₂H₁₇NO₄S
CAS No.:1610353-91-7
Molecular Formula:C₁₂H₁₇NO₄S
Molecular Weight:271.337
Hs Code.:

C<sub>12</sub>H<sub>17</sub>NO<sub>4</sub>S

Synonyms:C₁₂H₁₇NO₄S

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Chemical Property of C₁₂H₁₇NO₄S

Chemical Property:

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Technology Process of C₁₂H₁₇NO₄S

There total 5 articles about C₁₂H₁₇NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1610353-86-0
(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

: 1610353-91-7
C₁₂H₁₇NO₄S

: 1563551-09-6
C₁₂H₁₇NO₄S

Guidance literature:: carbon dioxide; With cesium fluoride; In Triethylene glycol dimethyl ether; under 7600.51 Torr;

(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine; In Triethylene glycol dimethyl ether; at 100 ℃; for 3h;

With hydrogenchloride; In Triethylene glycol dimethyl ether; water; pH=2;
DOI:10.1021/ol501143c

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1610353-59-7
(1R)-N-(tert-butylsulfonyl)-α-(dimethylphenylsilyl)benzylamine

: 1610353-91-7
C₁₂H₁₇NO₄S

: 1563551-09-6
C₁₂H₁₇NO₄S

Guidance literature:: carbon dioxide; With cesium fluoride; In N,N-dimethyl-formamide; at -20 ℃; for 0.25h; under 760.051 Torr;

(1R)-N-(tert-butylsulfonyl)-α-(dimethylphenylsilyl)benzylamine; In N,N-dimethyl-formamide; at -20 ℃; for 46h;

With hydrogenchloride; In water; N,N-dimethyl-formamide; pH=2; stereospecific reaction;
DOI:10.1021/ol501143c

Reference yield:

: 196929-85-8
(R)-N-benzylidene-2-methylpropane-2-sulfinamide

: 1610353-91-7
C₁₂H₁₇NO₄S

: 1563551-09-6
C₁₂H₁₇NO₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diethylzinc / tetrahydrofuran / 0.5 h / -78 °C

2.1: peracetic acid / dichloromethane / 0.33 h / 20 °C

3.1: cesium fluoride / Triethylene glycol dimethyl ether / 7600.51 Torr

3.2: 3 h / 100 °C

3.3: pH 2

With peracetic acid; n-butyllithium; diethylzinc; cesium fluoride; In tetrahydrofuran; Triethylene glycol dimethyl ether; dichloromethane;
DOI:10.1021/ol501143c