15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene

Base Information

• Chemical Name: 15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene
• CAS No.: 79965-52-9
• Molecular Formula: C₂₄H₂₀
• Molecular Weight: 308.423

Synonyms:15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene

Chemical Property of 15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene

There total 3 articles about 15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

15-phenyl-16-(phenylsulfonyl)tetracyclo[6.6.2.02,7.09,14]hexadeca-2(7),3,5,9(14),10,12,15-heptaene (132555-65-8) + ethyl iodide (75-03-6) → 15-ethyl-16-phenyltetracyclo[6.6.2.02,7.09,14]hexadeca-2(7),3,5,9(14),10,12,15-heptaene (79965-52-9)

Guidance literature:

With n-butyllithium; In diethyl ether; for 6h; Heating;

DOI:10.1021/ol016215a

Reference yield:

C18H16O (53483-00-4) → 15-ethyl-16-phenyltetracyclo[6.6.2.02,7.09,14]hexadeca-2(7),3,5,9(14),10,12,15-heptaene (79965-52-9)

Guidance literature:

With toluene-4-sulfonic acid; Multistep reaction; 2.) benzene, reflux;

DOI:10.1246/cl.1981.1241

Reference yield:

9,10-dihydro-9,10-ethano-anthracen-11-one (6372-63-0) → 15-ethyl-16-phenyltetracyclo[6.6.2.02,7.09,14]hexadeca-2(7),3,5,9(14),10,12,15-heptaene (79965-52-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.)LDA / THF, HMPA

2: 2.)TsOH / 2.) benzene, reflux

With toluene-4-sulfonic acid; lithium diisopropyl amide;

DOI:10.1246/cl.1981.1241

upstream raw materials:

C₁₈H₁₆O

15-phenyl-16-(phenylsulfonyl)tetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene

ethyl iodide

9,10-dihydro-9,10-ethano-anthracen-11-one

Downstream raw materials:

1-phenyl-1-butyne

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 79965-52-9 15-ethyl-16-phenyltetracyclo[6.6.2.0^2,7.0^9,14]hexadeca-2⁽⁷⁾,3,5,9⁽¹⁴⁾,10,12,15-heptaene

Send

Send

Metric Ton KG G Pound L ML

Send

Send