cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

Base Information

Chemical Name:cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester
CAS No.:461406-29-1
Molecular Formula:C₁₉H₃₄O₃Si
Molecular Weight:338.563
Hs Code.:

cyclohexanecarboxylic acid 3-(<i>tert</i>-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

Synonyms:cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

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Chemical Property of cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

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Technology Process of cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

There total 4 articles about cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 461406-44-0
[3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enyl]-methanol

: 98-89-5
Cyclohexanecarboxylic acid

: 461406-29-1
cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 23 ℃; for 1.5h;
DOI:10.1021/ol026260y

Reference yield:

: 162086-59-1
3-hydroxy-cyclopentene-1-carboxylic acid methyl ester

: 461406-29-1
cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.19 g / imidazole / dimethylformamide / 0.83 h / 23 °C

2: 86 percent / DIBAL-H / CH₂Cl₂; hexane / 0.33 h / -78 °C

3: 100 percent / DMAP; DCC / CH₂Cl₂ / 1.5 h / 23 °C

With 1H-imidazole; dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; In hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol026260y

Reference yield:

: 461406-43-9
3-(tert-Butyl-dimethyl-silanyloxy)-cyclopent-1-enecarboxylic acid methyl ester

: 461406-29-1
cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / DIBAL-H / CH₂Cl₂; hexane / 0.33 h / -78 °C

2: 100 percent / DMAP; DCC / CH₂Cl₂ / 1.5 h / 23 °C

With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; In hexane; dichloromethane;
DOI:10.1021/ol026260y