N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

Base Information

Chemical Name:N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide
CAS No.:1098209-30-3
Molecular Formula:C₁₇H₂₃ClFN₃O₂
Molecular Weight:355.84
Hs Code.:

N<SUP>1</SUP>-(4-chloro-3-fluorophenyl)-N<SUP>2</SUP>-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

Synonyms:N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

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Technology Process of N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

There total 3 articles about N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 36768-62-4
4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE

: 1226789-23-6
ethyl 2-((4-chloro-3-fluorophenyl)amino)-2-oxoacetate

: 1098209-30-3
N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

Guidance literature:: With triethylamine; In toluene; at 150 ℃; for 3h; Microwave irradiation;
DOI:10.3389/fphar.2020.613361

Reference yield:

: 367-22-6
4-chloro-3-fluoroaniline

: 1098209-30-3
N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 12 h / 0 - 20 °C

2: triethylamine / ethanol / 3 h / 150 °C / Microwave irradiation

With triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmc.2013.02.041

Reference yield:

: 372-19-0
meta-fluoroaniline

: 1098209-30-3
N¹-(4-chloro-3-fluorophenyl)-N²-(2,2,6,6-tetramethylpiperidin-4-yl) oxalamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-chloro-succinimide / chloroform / 42 h / 0 °C

2: triethylamine / tetrahydrofuran / 12 h / 0 - 20 °C

3: triethylamine / ethanol / 3 h / 150 °C / Microwave irradiation

With N-chloro-succinimide; triethylamine; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.bmc.2013.02.041