Technology Process of C45H54N2O13
There total 6 articles about C45H54N2O13 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C
2: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 10 h / 20 °C
3: pyridine / 40 h / 20 °C
With
magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; pyridine; diethyl ether; nitromethane;
DOI:10.1016/j.carres.2012.04.010
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / 48 h / 20 °C
2.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C
2.2: solid phase reaction
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 48 h / 20 °C
4.1: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 10 h / 20 °C
5.1: pyridine / 40 h / 20 °C
With
magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride; sulfur trioxide trimethylamine complex;
In
tetrahydrofuran; pyridine; diethyl ether; nitromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010