C₄₄H₆₉IO₃

Base Information

• Chemical Name: C₄₄H₆₉IO₃
• CAS No.: 1207158-64-2
• Molecular Formula: C₄₄H₆₉IO₃
• Molecular Weight: 772.935
• Mol file: 1207158-64-2.mol

Synonyms:C₄₄H₆₉IO₃

Chemical Property of C₄₄H₆₉IO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₆₉IO₃

There total 4 articles about C₄₄H₆₉IO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

p-Iodophenol (540-38-5) + Chol-(CH2)3-Br (82962-34-3) → C44H69IO3 (1207158-64-2)

Guidance literature:

With potassium carbonate; In acetone; for 12h; Reflux;

DOI:10.1016/j.tetlet.2009.11.066

Reference yield:

11-bromoundecanoyl chloride (15949-84-5) → C44H69IO3 (1207158-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 12 h / 20 °C

2: potassium carbonate / acetone / 12 h / Reflux

With pyridine; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1080/15421406.2013.779180

Reference yield:

cholesterol (57-88-5) → C44H69IO3 (1207158-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 12 h / 20 °C

2: potassium carbonate / acetone / 12 h / Reflux

With pyridine; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1080/15421406.2013.779180

upstream raw materials:

p-Iodophenol

Chol-(CH₂)₃-Br

11-bromoundecanoyl chloride

cholesterol

Downstream raw materials:

C₅₂H₇₆N₂O₅

C₅₃H₇₈N₂O₅