N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Base Information

Chemical Name:N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide
CAS No.:1313374-17-2
Molecular Formula:C₁₅H₂₃NO₂
Molecular Weight:249.353
Hs Code.:

Synonyms:N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Suppliers and Price of N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Chemical Property:

Purity/Quality:: ≥99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

There total 17 articles about N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313429-30-9
2-methyl-3-(3-methoxyphenyl)valeryl chloride

: 124-40-3
dimethyl amine

: 1313374-17-2
N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Guidance literature:: With sodium carbonate; In water; toluene; at 0 - 5 ℃; for 1h;

Reference yield:

: 1313429-17-2
3-(1-bromopropyl)anisole

: 1313374-17-2
N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 3 h / 25 °C

2.1: sodium hydride / toluene / 1 h / 20 °C / Inert atmosphere

2.2: 4 h / 45 - 50 °C

2.3: 0 - 5 °C / pH 1

3.1: lithium chloride / dimethyl sulfoxide / 15 h / 150 - 160 °C

4.1: sodium hydroxide / ethylene glycol / 4 h / 170 - 180 °C

4.2: pH 1

5.1: thionyl chloride / toluene / 3 h / 75 - 80 °C

6.1: sodium carbonate / toluene; water / 1 h / 0 - 5 °C

With thionyl chloride; sodium hydride; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; sodium hydroxide; In water; ethylene glycol; dimethyl sulfoxide; toluene;

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 1313374-17-2
N,N-dimethyl-2-methyl-3-(3-methoxyphenyl)valeramide

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 6 h / 50 - 60 °C

2.1: tetrahydrofuran / -15 - 25 °C / Inert atmosphere

2.2: 0 - 5 °C

3.1: sodium hydride / toluene / 1 h / 20 °C / Inert atmosphere

3.2: 4 h / 45 - 50 °C

3.3: 0 - 5 °C / pH 1

4.1: lithium chloride / dimethyl sulfoxide / 15 h / 150 - 160 °C

5.1: sodium hydroxide / ethylene glycol / 4 h / 170 - 180 °C

5.2: pH 1

6.1: thionyl chloride / toluene / 3 h / 75 - 80 °C

7.1: sodium carbonate / toluene; water / 1 h / 0 - 5 °C

With thionyl chloride; sodium hydride; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; sodium hydroxide; In tetrahydrofuran; water; ethylene glycol; dimethyl sulfoxide; toluene;