C₁₉H₂₇Cl₃N₂O₅*ClH

Base Information

Chemical Name:C₁₉H₂₇Cl₃N₂O₅*ClH
CAS No.:90195-07-6
Molecular Formula:C₁₉H₂₇Cl₃N₂O₅*ClH
Molecular Weight:506.254
Hs Code.:

C<sub>19</sub>H<sub>27</sub>Cl<sub>3</sub>N<sub>2</sub>O<sub>5</sub>*ClH

Synonyms:C₁₉H₂₇Cl₃N₂O₅*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₂₇Cl₃N₂O₅*ClH

Chemical Property:

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Technology Process of C₁₉H₂₇Cl₃N₂O₅*ClH

There total 2 articles about C₁₉H₂₇Cl₃N₂O₅*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 90195-01-0
L-N⁽²⁾-Boc-N⁽⁵⁾-trOC-N⁽⁵⁾-benzyloxyornithine tert-butyl ester

: 90195-07-6
C₁₉H₂₇Cl₃N₂O₅*ClH

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 24h; Ambient temperature;
DOI:10.1021/jo00187a023

Reference yield:

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 90195-07-6
C₁₉H₂₇Cl₃N₂O₅*ClH

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NEt₃, 2.) NaBH₄ / 1.) THF, 1 h, -5 deg C, 2.) H₂O, 4 h, 0 deg C -> room temperature

2: 80 percent / PPh₃, DEAD / tetrahydrofuran / 16 h / Ambient temperature

3: 80 percent / HCl / ethyl acetate / 24 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/jo00187a023

Reference yield:

: 90195-07-6
C₁₉H₂₇Cl₃N₂O₅*ClH

: 18928-00-2
N,N’-{[(2S,5S)-3,6-dioxopiperazine-2,5-diyl]bis(propane-3,1-diyl)}bis(N-hydroxyacetamide)

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / 2 h / Heating

2: 70 percent / 2-ethoxy-N-(ethoxycarbonyl)-1,2-dihydroquinoline (EEDQ), NEt₃ / acetonitrile / 16 h / Ambient temperature

3: 1.) HBr, 2.) NH₃ / 1.) AcOH, 20 min, room temperature, 2.) MeOH, several days, room temperature

4: 80 percent / Zn dust, acetic acid / 1 h / Ambient temperature

5: 70 percent / H₂ / 5percent Pd/C / methanol / 3 h / 760 Torr / Ambient temperature

With thionyl chloride; ammonia; hydrogen bromide; hydrogen; acetic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; zinc; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1021/jo00187a023