δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

Base Information

Chemical Name:δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride
CAS No.:90195-08-7
Molecular Formula:C₁₆H₂₁Cl₃N₂O₅*ClH
Molecular Weight:464.173
Hs Code.:

Synonyms:δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

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Chemical Property of δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

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Technology Process of δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

There total 8 articles about δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 67-56-1
methanol

: 90195-01-0
L-N⁽²⁾-Boc-N⁽⁵⁾-trOC-N⁽⁵⁾-benzyloxyornithine tert-butyl ester

: 90195-08-7
δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

Guidance literature:: With thionyl chloride; for 2h; Heating;
DOI:10.1021/jo00187a023

Reference yield: 60.0%

: 67-56-1
methanol

: 90195-05-4
C₁₅H₁₉Cl₃N₂O₅

: 90195-08-7
δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

Guidance literature:: With thionyl chloride; for 2h; Heating;
DOI:10.1021/jo00187a023

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 90195-08-7
δ-N-benzyloxy-δ-N-(2,2,2-trichloroethoxy)carbonyl-L-ornithine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / acetonitrile / 1 h / Ambient temperature

2: 80 percent / PPh₃, DEAD / tetrahydrofuran / 16 h / Ambient temperature

3: 65 percent / SOCl₂ / 2 h / Heating

With pyridine; thionyl chloride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00187a023