10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine

Base Information

Chemical Name:10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine
CAS No.:10464-35-4
Molecular Formula:C₁₄H₁₄N₂
Molecular Weight:210.279
Hs Code.:
DSSTox Substance ID:DTXSID60385385
Wikidata:Q82178134
ChEMBL ID:CHEMBL1329412
Mol file:10464-35-4.mol

Synonyms:10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine;10464-35-4;6,11-dihydro-5H-benzo[b][1]benzazepin-2-amine;Oprea1_077241;Oprea1_380003;CBDivE_009042;MLS000712642;CHEMBL1329412;SCHEMBL19224992;DTXSID60385385;HMS1648F17;HMS2671J19;STK386546;AKOS000549129;SMR000282409;A903701;SR-01000597327;SR-01000597327-1;2-azatricyclo[9.4.0.0?,?]pentadeca-1(15),3,5,7,11,13-hexaen-5-amine

Suppliers and Price of 10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
10,11-DIHYDRO-5H-DIBENZ[B,F]AZEPIN-3-AMINE 95.00%
5MG
$ 505.03

Total 6 raw suppliers

Chemical Property of 10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine

Chemical Property:

Melting Point:98-100 °C
Boiling Point:386.3±42.0 °C(Predicted)
PKA:5.14±0.20(Predicted)
Density:1.154±0.06 g/cm3(Predicted)
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:210.115698455
Heavy Atom Count:16
Complexity:241

Purity/Quality:

97% ^*data from raw suppliers

10,11-DIHYDRO-5H-DIBENZ[B,F]AZEPIN-3-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC=CC=C2NC3=C1C=CC(=C3)N

Technology Process of 10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine

There total 5 articles about 10,11-dihydro-5H-dibenzo[b,f]azepin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 84803-67-8
3-amino-5-acetyl-10,11-dihydro-5H-dibenzazepine

: 10464-35-4
3-amino-10,11-dihydro-5H-dibenzazepine

Guidance literature:: With potassium hydroxide; In propan-1-ol; for 5h; Heating;
DOI:10.1007/BF00766590

Reference yield:

: 494-19-9
9,10-dihydrodibenzazepine

: 10464-35-4
3-amino-10,11-dihydro-5H-dibenzazepine

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 2 h / 110 °C

2: sulfuric acid; nitric acid / 0.5 h / 0 °C

3: palladium on activated charcoal; hydrogen / methanol / 2 h / 20 °C

4: hydrogenchloride; acetic acid / water / Reflux

With hydrogenchloride; sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; acetic acid; In methanol; water;

Reference yield:

: 13080-75-6
5-acetyliminodibenzyl

: 10464-35-4
3-amino-10,11-dihydro-5H-dibenzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 0.5 h / 0 °C

2: palladium on activated charcoal; hydrogen / methanol / 2 h / 20 °C

3: hydrogenchloride; acetic acid / water / Reflux

With hydrogenchloride; sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; acetic acid; In methanol; water;