tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane
CAS No.:139140-12-8
Molecular Formula:C₂₀H₃₈O₃Si₂
Molecular Weight:382.691
Hs Code.:

Synonyms:tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

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Chemical Property of tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

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Technology Process of tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

There total 1 articles about tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 498-00-0
4-hydroxymethyl-2-methoxyphenol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 139140-12-8
tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 25 ℃; for 3h;

Reference yield: 95.0%

: 139140-12-8
tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

: 139140-16-2
4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenol

Guidance literature:: With CH₃O₃S^(1-)*C₂₇H₅₃N₂O₁₂⁽¹⁺⁾; cesium fluoride; In tert-Amyl alcohol; at 70 ℃; for 0.25h; chemoselective reaction;
DOI:10.1016/j.tetlet.2012.02.016

Reference yield: 95.0%

: 139140-12-8
tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane

: 74-88-4
methyl iodide

: 4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-1,2-dimethoxybenzene

Guidance literature:: tert-butyl(4-(tert-butyldimethylsilyloxy)-3-methoxybenzyloxy)dimethylsilane; With lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1055/s-2003-38744