3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester

Base Information

• Chemical Name: 3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester
• CAS No.: 129027-72-1
• Molecular Formula: C₁₃H₁₆ClN₃O₃
• Molecular Weight: 297.741

Synonyms:3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester

Chemical Property of 3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester

Chemical Property:

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Technology Process of 3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester

There total 1 articles about 3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-(4-chlorophenyl)acetic hydrazide (57676-51-4) + Ethyl 3-ethoxy-3-iminopropionate (27317-59-5) → 3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester (129027-72-1)

Guidance literature:

In ethanol; 1) 70-75 deg C, 1-2 min, 2) r.t., 2h;

DOI:10.1002/jhet.5570270337

Reference yield: 82.0%

3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester (129027-72-1) + ethyl (ethoxymethylene)cyanoacetate (94-05-3,42466-69-3) → 5-Amino-3-(4-chloro-benzyl)-[1,2,4]triazolo[4,3-a]pyridine-6,8-dicarboxylic acid diethyl ester (135449-25-1)

Guidance literature:

In dimethyl sulfoxide; toluene; for 0.5h; Heating;

Reference yield: 75.0%

3-Amino-3-{[2-(4-chloro-phenyl)-acetyl]-hydrazono}-propionic acid ethyl ester (129027-72-1) → 5-Amino-2-[2-(4-chloro-phenyl)-acetyl]-2,4-dihydro-pyrazol-3-one (129027-77-6)

Guidance literature:

With sodium; In ethanol; for 12h; Ambient temperature;

DOI:10.1002/jhet.5570270337

upstream raw materials:

2-(4-chlorophenyl)acetic hydrazide

Ethyl 3-ethoxy-3-iminopropionate

Downstream raw materials:

5-Amino-2-[2-(4-chloro-phenyl)-acetyl]-2,4-dihydro-pyrazol-3-one

2-[2-(4-Chloro-phenyl)-acetyl]-4-hydroxy-4-methyl-3a,4,5,6-tetrahydro-2H-pyrrolo[2,3-c]pyrazol-3-one

Ethyl 6-<2-(4-chlorophenylacetyl)hydrazino>-3-cyano-1,2-dihydro-2-oxo-5-pyridinecarboxylate

5-Amino-3-(4-chloro-benzyl)-[1,2,4]triazolo[4,3-a]pyridine-6,8-dicarboxylic acid diethyl ester

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