O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

Base Information

Chemical Name:O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate
CAS No.:1346434-21-6
Molecular Formula:C₃₀H₃₂ClN₅O₃
Molecular Weight:546.069
Hs Code.:

Synonyms:O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

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Chemical Property of O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

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Technology Process of O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

There total 11 articles about O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1346434-20-5
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

: 1346434-21-6
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

Guidance literature:: With chloro-trimethyl-silane; In tetrahydrofuran;

Reference yield:

: O-(9-(2-((N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

: 1346434-21-6
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: chloro-trimethyl-silane / tetrahydrofuran

With chloro-trimethyl-silane; In tetrahydrofuran;

Reference yield:

: 1346434-76-1
2-((N-tBOC-N-methylamino)methyl)-fluorene-9-carboxaldehyde

: 1346434-21-6
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenyl-N-chloromethylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium tetrahydroborate / methanol

2: pyridine / tetrahydrofuran / 1 h / 20 °C / Cooling with ice

3: sodium hydrogencarbonate; water / acetone / 0.5 h

4: trifluoroacetic acid

5: tetrahydrofuran

6: chloro-trimethyl-silane / tetrahydrofuran

With pyridine; sodium tetrahydroborate; chloro-trimethyl-silane; water; sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; acetone;