O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

Base Information

Chemical Name:O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate
CAS No.:1346434-20-5
Molecular Formula:C₂₉H₃₁N₅O₃
Molecular Weight:497.597
Hs Code.:

Synonyms:O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

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Chemical Property of O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

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Technology Process of O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

There total 11 articles about O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: O-(9-(2-((N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

: 1293300-31-8
N-(6-azidohexanoyl)succinimide

: 1346434-20-5
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran;

Reference yield:

: 866363-70-4
6-azidohexanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: O-(9-(2-((N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

: 1346434-20-5
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

Guidance literature:: In tetrahydrofuran;

Reference yield:

: 1346434-17-0
2-((N-tBOC-N-methylamino)methyl)fluorene

: 1346434-20-5
O-(9-(2-((N-(6-azidohexanoyl)-N-methylamino)methyl)fluorenyl)methyl) N-phenylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: sodium tetrahydroborate / methanol

3.1: pyridine / tetrahydrofuran / 1 h / 20 °C / Cooling with ice

4.1: sodium hydrogencarbonate; water / acetone / 0.5 h

5.1: trifluoroacetic acid

6.1: tetrahydrofuran

With pyridine; sodium tetrahydroborate; water; sodium hydrogencarbonate; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; acetone;