1-(4-methoxyphenyl)-N₁-(phenylmethyl)-1,2-ethanediamine dihydrochloride

Base Information

• Chemical Name: 1-(4-methoxyphenyl)-N₁-(phenylmethyl)-1,2-ethanediamine dihydrochloride
• CAS No.: 40658-73-9
• Molecular Formula: C₁₆H₂₂N₂O*2Cl
• Molecular Weight: 329.269
• Mol file: 40658-73-9.mol

Synonyms:1-(4-methoxyphenyl)-N₁-(phenylmethyl)-1,2-ethanediamine dihydrochloride

Chemical Property of 1-(4-methoxyphenyl)-N₁-(phenylmethyl)-1,2-ethanediamine dihydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-(4-methoxyphenyl)-N₁-(phenylmethyl)-1,2-ethanediamine dihydrochloride

There total 1 articles about 1-(4-methoxyphenyl)-N₁-(phenylmethyl)-1,2-ethanediamine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(N-benzylamino)-2-(4-methoxyphenyl)acetonitrile (65551-44-2) → 1-(4-methoxyphenyl)-N1-(phenylmethyl)-1,2-ethanediamine dihydrochloride (40658-73-9)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃;

DOI:10.1016/j.saa.2007.02.011

Reference yield:

copper(II) perchlorate hexahydrate + 1-(4-methoxyphenyl)-N1-(phenylmethyl)-1,2-ethanediamine dihydrochloride (40658-73-9) + 1-phenylbutan-1,3-dione (93-91-4) → [Cu(2-amino-1-benzylamino-1-(4-methoxyphenyl)ethane(-1H))(benzoylacetonato)(H2O)](ClO4)

Guidance literature:

In ethanol; benzoylacetone added to soln. of diamine*2HCl in EtOH, soln. of Cu(ClO4)2*6H2O in EtOH added, mixt. refluxed for 30 min; pptn. by addn. of dilute NH4OH, solid sepd. and washed with EtOH, dried;elem. anal.;

DOI:10.1016/j.saa.2007.02.011

Reference yield:

copper(II) perchlorate hexahydrate + 1-(4-methoxyphenyl)-N1-(phenylmethyl)-1,2-ethanediamine dihydrochloride (40658-73-9) + acetylacetone (123-54-6,81235-32-7) → [Cu(2-amino-1-benzylamino-1-(4-methoxyphenyl)ethane(-1H))(acetylacetonato)(H2O)](ClO4)

Guidance literature:

In ethanol; acetylacetone added to soln. of diamine*2HCl in EtOH, soln. of Cu(ClO4)2*6H2O in EtOH added, mixt. refluxed for 30 min; pptn. by addn. of dilute NH4OH, solid sepd. and washed with EtOH, dried;elem. anal.;

DOI:10.1016/j.saa.2007.02.011

upstream raw materials:

2-(N-benzylamino)-2-(4-methoxyphenyl)acetonitrile