[naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester

Base Information

• Chemical Name: [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester
• CAS No.: 415726-50-0
• Molecular Formula: C₂₃H₂₄N₂O₇S
• Molecular Weight: 472.519

Synonyms:[naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester

Chemical Property of [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester

Chemical Property:

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Technology Process of [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester

There total 4 articles about [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-naphthalene methanol (4780-79-4) + tert-butyl 2-((2-nitrophenylsulfonamido)-oxy)acetate (415726-51-1) → [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester (415726-50-0)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ol010251s

Reference yield:

2-Nitrobenzenesulfonyl chloride (1694-92-4) → [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester (415726-50-0)

Guidance literature:

Multi-step reaction with 2 steps

1: collidine / dimethylformamide / 1.5 h / 20 °C

2: 92 percent / PPh₃; DIAD / CH₂Cl₂ / 1 h / 20 °C

With 2,3,5-trimethyl-pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ol010251s

Reference yield:

tert-butyl aminooxyacetate (56834-02-7) → [naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetic acid tert-butyl ester (415726-50-0)

Guidance literature:

Multi-step reaction with 2 steps

1: collidine / dimethylformamide / 1.5 h / 20 °C

2: 92 percent / PPh₃; DIAD / CH₂Cl₂ / 1 h / 20 °C

With 2,3,5-trimethyl-pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ol010251s

upstream raw materials:

1-naphthalene methanol

tert-butyl 2-((2-nitrophenylsulfonamido)-oxy)acetate

2-Nitrobenzenesulfonyl chloride

tert-butyl aminooxyacetate

Downstream raw materials:

(methyl-{[naphthalen-1-ylmethyl-(2-nitro-benzenesulfonyl)-aminooxy]-acetyl}-aminooxy)-acetic acid tert-butyl ester

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