Phenyl-2-(2-naphthyl)-vinyl-methanol

Base Information

Chemical Name:Phenyl-2-(2-naphthyl)-vinyl-methanol
CAS No.:56345-33-6
Molecular Formula:C₁₉H₁₆O
Molecular Weight:260.335
Hs Code.:

Synonyms:Phenyl-2-(2-naphthyl)-vinyl-methanol

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Chemical Property of Phenyl-2-(2-naphthyl)-vinyl-methanol

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Technology Process of Phenyl-2-(2-naphthyl)-vinyl-methanol

There total 14 articles about Phenyl-2-(2-naphthyl)-vinyl-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 944551-29-5
3-(naphthalen-2-yl)-1-phenylprop-2-yn-1-ol

: 56345-33-6
(E)-3-(naphthalen-2-yl)-1-phenylprop-2-en-1-ol

Guidance literature:: 3-(naphthalen-2-yl)-1-phenylprop-2-yn-1-ol; With sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; toluene; at 0 ℃; for 4h; Inert atmosphere;

With hydrogenchloride; In diethyl ether; water; toluene; at 0 ℃; Inert atmosphere;
DOI:10.1039/c3ob41857j

Reference yield:

: 53744-33-5,42299-50-3
3-(2-naphthalenyl)-1-phenylprop-2-en-1-one

: 56345-33-6
Phenyl-2-(2-naphthyl)-vinyl-methanol

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In methanol; at 0 - 20 ℃; for 0.5h;
DOI:10.1002/adsc.202100272

Reference yield:

: 100-52-7
benzaldehyde

: 56345-33-6
(E)-3-(naphthalen-2-yl)-1-phenylprop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / dichloromethane / 3 h / Inert atmosphere

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene; diethyl ether / 4 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1039/c3ob41857j