diphenoxyphosphoryl(dihydroxyphosphoryl)imide

Base Information

• Chemical Name: diphenoxyphosphoryl(dihydroxyphosphoryl)imide
• CAS No.: 74203-77-3
• Molecular Formula: C₁₂H₁₃NO₆P₂
• Molecular Weight: 329.186
• Mol file: 74203-77-3.mol

Synonyms:diphenoxyphosphoryl(dihydroxyphosphoryl)imide

Chemical Property of diphenoxyphosphoryl(dihydroxyphosphoryl)imide

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of diphenoxyphosphoryl(dihydroxyphosphoryl)imide

There total 7 articles about diphenoxyphosphoryl(dihydroxyphosphoryl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

O,O-diphenyl (N-dichlorophosphorylimido)chlorophosphate (75944-09-1) → diphenoxyphosphoryl(dihydroxyphosphoryl)imide (74203-77-3)

Guidance literature:

With water; at 20 ℃; for 48h;

DOI:10.1007/BF00955310

Reference yield:

phenol (108-95-2,27073-41-2) → diphenoxyphosphoryl(dihydroxyphosphoryl)imide (74203-77-3)

Guidance literature:

Multi-step reaction with 4 steps

1: phosphoryl chloride / magnesium dichloride / 2 h / Heating

2: ammonia / ethanol

3: phosphorus pentachloride / 1.) 15-25 deg C, 5-6 h, 2.) 50-60 deg C, 30 min

4: water

With phosphorus pentachloride; ammonia; water; trichlorophosphate; magnesium chloride; In ethanol;

DOI:10.1246/bcsj.63.1243

Reference yield:

chlorophosphoric acid diphenyl ester (2524-64-3) → diphenoxyphosphoryl(dihydroxyphosphoryl)imide (74203-77-3)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonia / H₂O; ethanol

2: 1.) PCl₅

3: H₂O

With phosphorus pentachloride; ammonia; water; In ethanol; water;

DOI:10.1007/BF00957317

upstream raw materials:

(diphenoxyphosphorylimido)trichlorophosphate

O,O-diphenyl (N-dichlorophosphorylimido)chlorophosphate

diphenylphosphoroamidate

chlorophosphoric acid diphenyl ester