(diphenoxyphosphorylimido)trichlorophosphate

Base Information

• Chemical Name: (diphenoxyphosphorylimido)trichlorophosphate
• CAS No.: 16698-78-5
• Molecular Formula: C₁₂H₁₀Cl₃NO₃P₂
• Molecular Weight: 384.523
• Mol file: 16698-78-5.mol

Synonyms:

Chemical Property of (diphenoxyphosphorylimido)trichlorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (diphenoxyphosphorylimido)trichlorophosphate

There total 3 articles about (diphenoxyphosphorylimido)trichlorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenol (108-95-2,27073-41-2) → (diphenoxyphosphorylimido)trichlorophosphate (16698-78-5)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphoryl chloride / magnesium dichloride / 2 h / Heating

2: ammonia / ethanol

3: phosphorus pentachloride / 1.) 15-25 deg C, 5-6 h, 2.) 50-60 deg C, 30 min

With phosphorus pentachloride; ammonia; trichlorophosphate; magnesium chloride; In ethanol;

DOI:10.1246/bcsj.63.1243

Reference yield:

chlorophosphoric acid diphenyl ester (2524-64-3) → (diphenoxyphosphorylimido)trichlorophosphate (16698-78-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonia / ethanol

2: phosphorus pentachloride / 1.) 15-25 deg C, 5-6 h, 2.) 50-60 deg C, 30 min

With phosphorus pentachloride; ammonia; In ethanol;

DOI:10.1246/bcsj.63.1243

Reference yield:

diphenylphosphoroamidate (2015-56-7) → (diphenoxyphosphorylimido)trichlorophosphate (16698-78-5)

Guidance literature:

With phosphorus pentachloride;

upstream raw materials:

diphenylphosphoroamidate

chlorophosphoric acid diphenyl ester

phenol

Downstream raw materials:

diphenoxyphosphoryl-[tris-(4-nitro-phenoxy)-phosphoranyliden]-amine

diphenoxyphosphoryl-triphenoxyphosphoranyliden-amine

diphenoxyphosphoryl(dihydroxyphosphoryl)imide

dichlorophosphoryl-diphenoxyphosphoryl-amine