(2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol

Base Information

Chemical Name:(2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol
CAS No.:1088779-94-5
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:

Synonyms:(2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol

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Chemical Property of (2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol

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Technology Process of (2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol

There total 1 articles about (2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1088779-95-6
(E)-(5S,7S,8S)-9-(benzyloxy)-5,7-dihydroxy-8-methylnon-2-enal

: 762-72-1
allyl-trimethyl-silane

: 1088779-94-5
(2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol

: C₂₀H₂₈O₃

Guidance literature:: With indium(III) bromide; In dichloromethane; at 25 ℃; for 1h; optical yield given as %de;
DOI:10.1055/s-2008-1067219

Reference yield: 92.0%

: 1088779-94-5
(2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol

: 74-88-4
methyl iodide

: 1088779-99-0
(2S,6R)-6-allyl-2-[(2S,3S)-4-(benzyloxy)-2-methoxy-3-methylbutyl]-3,6-dihydro-2H-pyran

Guidance literature:: (2S,3S)-1-[(2S,6R)-6-allyl-3,6-dihydro-2H-pyran-2-yl]-4-(benzyloxy)-3-methylbutan-2-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.25h;

methyl iodide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 25 ℃; for 4h;
DOI:10.1055/s-2008-1067219