Technology Process of C11H12N4O
There total 4 articles about C11H12N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium acetate; copper(II) bis(trifluoromethanesulfonate); 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
Reagent/catalyst;
Time;
Inert atmosphere;
DOI:10.1021/ol403687k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: indium / tetrahydrofuran; water / 20 °C / Inert atmosphere
2: Jones reagent / diethyl ether / 0 - 20 °C / Inert atmosphere
3: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere
4: 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one; copper(II) bis(trifluoromethanesulfonate); sodium acetate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
With
indium; Jones reagent; hydroxylamine hydrochloride; sodium acetate; copper(II) bis(trifluoromethanesulfonate); 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one;
In
tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol403687k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Jones reagent / diethyl ether / 0 - 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere
3: 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one; copper(II) bis(trifluoromethanesulfonate); sodium acetate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
With
Jones reagent; hydroxylamine hydrochloride; sodium acetate; copper(II) bis(trifluoromethanesulfonate); 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one;
In
diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol403687k