(2-(bromomethyl)benzyloxy)(tert-butyl)dimethylsilane

Base Information

• Chemical Name: (2-(bromomethyl)benzyloxy)(tert-butyl)dimethylsilane
• CAS No.: 148671-87-8
• Molecular Formula: C₁₄H₂₃BrOSi
• Molecular Weight: 315.326
• Mol file: 148671-87-8.mol

Synonyms:1-(bromomethyl)-2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>benzene

Chemical Property of (2-(bromomethyl)benzyloxy)(tert-butyl)dimethylsilane

Chemical Property:

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Technology Process of (2-(bromomethyl)benzyloxy)(tert-butyl)dimethylsilane

There total 5 articles about (2-(bromomethyl)benzyloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

t-butyldimethylsiyl triflate (69739-34-0) + (2-(bromomethyl)phenyl)methanol (74785-02-7) → 1-(bromomethyl)-2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>benzene (148671-87-8)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.7b01666

Reference yield: 74.0%

2-(tert-butyldimethylsiloxymethyl)benzyl alcohol (81168-17-4) → 1-(bromomethyl)-2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>benzene (148671-87-8)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1021/jo702052b

Reference yield:

2,6-dimethylpyridine (108-48-5) + t-butyldimethylsiyl triflate (69739-34-0) → 1-(bromomethyl)-2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>benzene (148671-87-8)

Guidance literature:

In dichloromethane;

upstream raw materials:

2,6-dimethylpyridine

t-butyldimethylsiyl triflate

2-(tert-butyldimethylsiloxymethyl)benzyl alcohol

(2-(bromomethyl)phenyl)methanol

Downstream raw materials:

1-{2-[(tert-butyldimethylsilanyloxy)methyl]benzyl}-1H-indole

1-{2-[(tert-butyldimethylsilanyloxy)methyl]benzyl}-1H-pyrrole

1-{2-[(tert-butyldimethylsilanyloxy)methyl]benzyl}-1H-indole-5-carboxylic acid methyl ester

tert-butyldimethyl((2-(4-(trimethylsilyl)but-3-yn-1-yl)benzyl)oxy)silane

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