3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

Base Information

Chemical Name:3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal
CAS No.:79801-71-1
Molecular Formula:C₁₆H₂₂O₃
Molecular Weight:262.349
Hs Code.:

Synonyms:3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

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Chemical Property of 3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

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Technology Process of 3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

There total 8 articles about 3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 79801-65-3
cybrodol methyl ether

: 79801-71-1
3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

Guidance literature:: With manganese(IV) oxide; In dichloromethane; Ambient temperature;
DOI:10.1139/v81-311

Reference yield:

: 74973-56-1
2-(4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 79801-71-1
3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / nitromethane / 0.5 h / 0 °C

2: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

3: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

4: 67 percent / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

5: 100 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

With manganese(IV) oxide; n-butyllithium; sulfuric acid; bromine; pyridinium p-toluenesulfonate; In tetrahydrofuran; nitromethane; dichloromethane; acetone;
DOI:10.1139/v81-311

Reference yield:

: 79801-57-3
2-(3-bromo-4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 79801-71-1
3-((3-(2-hydroxyethyl)-6-methoxymethyl-2,4-dimethyl)phenyl)-2-methyl-(E)-2-propenal

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

2: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

3: 67 percent / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

4: 100 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

With manganese(IV) oxide; n-butyllithium; sulfuric acid; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1139/v81-311