C₂₃H₃₇ClP₂Pd

Base Information

Chemical Name:C₂₃H₃₇ClP₂Pd
CAS No.:1429511-44-3
Molecular Formula:C₂₃H₃₇ClP₂Pd
Molecular Weight:517.367
Hs Code.:

C<sub>23</sub>H<sub>37</sub>ClP<sub>2</sub>Pd

Synonyms:C₂₃H₃₇ClP₂Pd

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Chemical Property of C₂₃H₃₇ClP₂Pd

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Technology Process of C₂₃H₃₇ClP₂Pd

There total 4 articles about C₂₃H₃₇ClP₂Pd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 13965-03-2
bis-triphenylphosphine-palladium(II) chloride

: 38177-85-4
1-(buta-1,3-diyn-1-yl)-4-methylbenzene

: 109-89-7
diethylamine

: 1429511-44-3
C₂₃H₃₇ClP₂Pd

Guidance literature:: With copper(l) chloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja5004747

Reference yield:

: 766-97-2
4-n-methylphenylacetylene

: 1429511-44-3
C₂₃H₃₇ClP₂Pd

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; silver nitrate / acetone / 1 h / 20 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 6 h / 55 °C / Inert atmosphere

3: potassium carbonate; methanol / dichloromethane / 1 h / 20 °C

4: copper(l) chloride / dichloromethane / 1 h / 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; potassium carbonate; silver nitrate; triethylamine; copper(l) chloride; In dichloromethane; acetone; 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ja5004747

Reference yield:

: 33491-05-3
1-(2-bromoethynyl)-4-methylbenzene

: 1429511-44-3
C₂₃H₃₇ClP₂Pd

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 6 h / 55 °C / Inert atmosphere

2: potassium carbonate; methanol / dichloromethane / 1 h / 20 °C

3: copper(l) chloride / dichloromethane / 1 h / 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; copper(l) chloride; In dichloromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja5004747