C₂₀H₂₇N₅O₂

Base Information

Chemical Name:C₂₀H₂₇N₅O₂
CAS No.:1558038-70-2
Molecular Formula:C₂₀H₂₇N₅O₂
Molecular Weight:369.467
Hs Code.:

C<sub>20</sub>H<sub>27</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:C₂₀H₂₇N₅O₂

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Chemical Property of C₂₀H₂₇N₅O₂

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Technology Process of C₂₀H₂₇N₅O₂

There total 7 articles about C₂₀H₂₇N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1558038-69-9
C₂₅H₃₃N₅O₃

: 1558038-70-2
C₂₀H₂₇N₅O₂

Guidance literature:: C₂₅H₃₃N₅O₃; With hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); In ethanol; water; at 80 ℃; for 72h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 114214-71-0
tert-butyl 3-methylidenepyrrolidine-1-carboxylate

: 1558038-70-2
C₂₀H₂₇N₅O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc/copper couple / diethyl ether; 1,2-dimethoxyethane / 48 h / 10 - 20 °C / Inert atmosphere

2.1: zinc; ammonium chloride / methanol / 8 h / 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran / 6 h / 0 - 20 °C

4.1: pyridine / dichloromethane / 0 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C

6.1: hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / water; ethanol / 72 h / 80 °C

6.2: 1 h / 20 °C

With pyridine; sodium tetrahydroborate; hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); zinc/copper couple; sodium hydride; ammonium chloride; zinc; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1239319-91-5
2-hydroxy-7-azaspiro[3.4]octane-7-carboxylic acid tert-butyl ester

: 1558038-70-2
C₂₀H₂₇N₅O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 0 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C

3.1: hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / water; ethanol / 72 h / 80 °C

3.2: 1 h / 20 °C

With pyridine; hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); sodium hydride; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;