4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

Base Information

Chemical Name:4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate
CAS No.:1448297-14-0
Molecular Formula:C₂₇H₂₈N₂O₉S₃
Molecular Weight:620.725
Hs Code.:

Synonyms:4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

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Chemical Property of 4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

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Technology Process of 4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

There total 4 articles about 4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448297-21-9
4-[(2-butyl-5-amino-1-benzofuran-3-yl)carbonyl]phenyl-4-aminobenzenesulfonate

: 124-63-0
methanesulfonyl chloride

: 1448297-14-0
4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 30 - 35 ℃; for 5h;

Reference yield:

: 141645-16-1
2-n-butyl-3-(4-hydroxybenzoyl)-5-nitrobenzofuran

: 1448297-14-0
4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 5.5 h / 20 °C / Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol / 7 h / 75 °C / 7500.75 Torr

3: pyridine / dichloromethane / 5 h / 30 - 35 °C

With pyridine; palladium 10% on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane;

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1448297-14-0
4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyl-4-[(methylsulfonyl)amino]benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 5.5 h / 20 °C / Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol / 7 h / 75 °C / 7500.75 Torr

3: pyridine / dichloromethane / 5 h / 30 - 35 °C

With pyridine; palladium 10% on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane;