4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

Base Information

Chemical Name:4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde
CAS No.:161403-53-8
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

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Chemical Property of 4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

Chemical Property:

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Technology Process of 4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

There total 5 articles about 4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36838-71-8
4-methylene-tetrahydro-pyran

: 161403-53-8
4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / Br₂ / CCl₄

2: K₂CO₃ / butan-2-one / 24 h / Heating

3: KOH / ethanol / 8 h / Heating

4: diethyl ether

5: dimethylformamide / 8 h / Heating

With potassium hydroxide; bromine; potassium carbonate; In tetrachloromethane; diethyl ether; ethanol; N,N-dimethyl-formamide; butanone;
DOI:10.1007/BF01169631

Reference yield:

: 79862-93-4
4-bromo-4-bromomethyltetrahydropyran

: 161403-53-8
4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / butan-2-one / 24 h / Heating

2: KOH / ethanol / 8 h / Heating

3: diethyl ether

4: dimethylformamide / 8 h / Heating

With potassium hydroxide; potassium carbonate; In diethyl ether; ethanol; N,N-dimethyl-formamide; butanone;
DOI:10.1007/BF01169631

Reference yield:

: 139091-97-7
4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>acetanilide

: 161403-53-8
4-<(5,6-dihydro-2H-pyran-4-yl)methyloxy>phenylcarbamoylmethyloxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 8 h / Heating

2: diethyl ether

3: dimethylformamide / 8 h / Heating

With potassium hydroxide; In diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1007/BF01169631