10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate

Base Information

Chemical Name:10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate
CAS No.:723752-25-8
Molecular Formula:C₂₆H₂₃NO₅
Molecular Weight:429.472
Hs Code.:

Synonyms:10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate

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Chemical Property of 10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate

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Technology Process of 10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate

There total 3 articles about 10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 98-88-4
benzoyl chloride

: 17388-17-9
(+/-)-nandinine

: 723752-25-8
10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate

Guidance literature:: With dmap; triethylamine; In chloroform; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.11.002

Reference yield:

: 2,3-methenedioxy-9-benzoxy-10-methoxyprotoberberine chloride

: 723752-25-8
10-methoxy-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinolin-9-yl benzoate

Guidance literature:: 2,3-methenedioxy-9-benzoxy-10-methoxyprotoberberine chloride; With sodium tetrahydroborate; at 60 ℃; for 0.25h;

With water;