4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester

Base Information

• Chemical Name: 4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester
• CAS No.: 86223-93-0
• Molecular Formula: C₁₂H₁₂N₄O₆S
• Molecular Weight: 340.316

Synonyms:4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester

Chemical Property of 4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester

Chemical Property:

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Technology Process of 4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester

There total 1 articles about 4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

3-nitro-4-chloro-5-N,N-dimethylaminomethyleneaminosulphonyl-benzoic acid methyl ester (60376-77-4) + copper(I) cyanide (544-92-3) → 4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester (86223-93-0)

Guidance literature:

In N,N-dimethyl-formamide; for 3.5h; Heating;

DOI:10.1002/ardp.19833160515

Reference yield: 78.0%

4-Cyano-3-dimethylaminomethylenaminosulfonyl-5-nitrobenzoesaeuremethylester (86223-93-0) → 4-Cyano-3-nitro-5-sulfamoylbenzoesaeuremethylester (86223-94-1)

Guidance literature:

With sulfuric acid; In methanol; for 24h; Heating;

DOI:10.1002/ardp.19833160515

upstream raw materials:

3-nitro-4-chloro-5-N,N-dimethylaminomethyleneaminosulphonyl-benzoic acid methyl ester

copper(I) cyanide

Downstream raw materials:

4-Cyano-3-nitro-5-sulfamoylbenzoesaeuremethylester

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