7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

Base Information

Chemical Name:7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III
CAS No.:156940-38-4
Molecular Formula:C₃₅H₃₈Cl₆O₁₅
Molecular Weight:911.396
Hs Code.:

Synonyms:7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

Suppliers and Price of 7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

There total 1 articles about 7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 145533-34-2
14-β-hydroxy-10-deacetylbaccatin III

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 156940-38-4
7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

Guidance literature:: With pyridine; at 80 ℃; for 5h;
DOI:10.1021/jm00036a004

Reference yield: 39.0%

: 156940-38-4
7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

: C₃₅H₃₆Cl₆O₁₅

: C₃₅H₃₄Cl₆O₁₅

Guidance literature:: With manganese(IV) oxide; In dichloromethane; ethyl acetate; for 24h; Ambient temperature;
DOI:10.1016/S0040-4039(00)78269-4

Reference yield:

: 156940-38-4
7,10-di-(2,2,2-trichloroethoxycarbonyl) 14β-hydroxy-10-deacetylbaccatin III

: C₄₉H₅₇NO₁₄

Guidance literature:: Multi-step reaction with 2 steps

1: NaHMDS / -40 °C

2: 72 percent / Zn, AcOH / methanol / 9 h / 40 °C

With sodium hexamethyldisilazane; acetic acid; zinc; In methanol;
DOI:10.1021/jm00036a004