S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

Base Information

Chemical Name:S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine
CAS No.:625124-00-7
Molecular Formula:C₅₂H₅₇ClN₂O₂S₂
Molecular Weight:841.622
Hs Code.:

Synonyms:S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

Chemical Property:

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Technology Process of S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

There total 4 articles about S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 109-70-6
1.3-chlorobromopropane

: 549514-84-3
tert-butyl 2-(tritylthio) ethyl (2-(2-(tritylthio)ethylamino)ethyl)carbamate

: 625124-00-7
S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; Heating;
DOI:10.1002/jlcr.698

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 625124-00-7
S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: natrium / liquid ammonia

1.2: trifluoroacetic acid

2.1: DIEA / acetonitrile

With sodium; N-ethyl-N,N-diisopropylamine; In ammonia; acetonitrile;
DOI:10.1016/S0040-4039(03)00224-7

Reference yield:

: 549514-83-2
S,S'-bis-triphenylmethyl-1,2-ethylenedicysteamine

: 625124-00-7
S,S'-bis-triphenylmethyl-N-(tert-butoxycarbonyl)-N'-(3-chloropropyl)-1,2-ethylenedicysteamine

Guidance literature:: Multi-step reaction with 2 steps

1: DIEA / acetonitrile

With N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1016/S0040-4039(03)00224-7