S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

Base Information

Chemical Name:S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate
CAS No.:1433278-90-0
Molecular Formula:C₂₄H₂₈OS₃
Molecular Weight:428.684
Hs Code.:

Synonyms:S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

Suppliers and Price of S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

There total 2 articles about S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 947536-19-8
2-phenylmethylene-1,3-dithiane 1-oxide

: 1433278-50-2
C₁₃H₁₆S

: 1433278-90-0
S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

Guidance literature:: With water; copper(I) bromide; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201204072

Reference yield:

: 17590-58-8
2-benzylidene-1,3-dithiane

: 1433278-90-0
S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / -20 - 25 °C / Inert atmosphere

2: copper(I) bromide; water / 24 h / 100 °C / Inert atmosphere

With water; 3-chloro-benzenecarboperoxoic acid; copper(I) bromide; In dichloromethane; 2: |Pummerer Sulfoxide Rearrangement;
DOI:10.1002/chem.201204072

Reference yield: 77.0%

: 2-thienylzinc iodide-lithium chloride complex

: 1433278-90-0
S-butyl 3-(1,3-dithian-2-ylidene)-3-phenyl-2-(4-methylphenyl)propanethioate

: 1433278-85-3
C₂₄H₂₂OS₃

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; toluene; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201204072