10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene

Base Information

Chemical Name:10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene
CAS No.:80503-29-3
Molecular Formula:C₄₄H₃₄
Molecular Weight:562.754
Hs Code.:

Synonyms:10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene

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Technology Process of 10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene

There total 17 articles about 10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 85865-17-4
C₂₂H₁₇Li

: 776-74-9
Bromodiphenylmethane

: 632-50-8
1,1,2,2-tetraphenylethane

: 85882-73-1
9-Benzhydryl-10-(4-methyl-benzylidene)-9,10-dihydro-anthracene

: 85865-37-8
9-(2,2-Diphenyl-1-p-tolyl-ethyl)-anthracene

: 80503-29-3
10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene

Guidance literature:: In tetrahydrofuran; at -70 ℃; for 0.0833333h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; further solvent;
DOI:10.1021/ja00352a025

Reference yield: 34.0%

: 60-29-7,927820-24-4
diethyl ether

: 77032-89-4
(9-anthryl)-p-methylbenzyl chloride

: 80503-09-9
9-tert-butyl-10-p-methylbenzylidene-9,10-dihydroanthracene

: 80502-93-8
α-tert-butyl-10-p-methylbenzylanthracene

: 80503-38-4
9-(1-Ethoxy-ethyl)-10-(4-methyl-benzylidene)-9,10-dihydro-anthracene

: 80503-29-3
10-(9'-anthryl-p-methylbenzyl)-9-p-methylbenzylidene-9,10-dihydroanthracene

Guidance literature:: With methyllithium; In diethyl ether; at 0 ℃; for 2h; Further byproducts given. Yields of byproduct given;
DOI:10.1021/ja00370a032